ManuScript Details
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Paper Id:
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IJCIRAS1520
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Title:
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ADSORPTION OF LEAD IONS (PB2+) FROM AQUEOUS SOLUTION WITH TETRA-ETHYL ORTHOSILICATE MODIFIED SILICA-IRON OXIDE (SI-FE3O4)MAGNETIC NANO-ADSORBENT.
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| Published in: |
International Journal Of Creative and Innovative Research In All Studies |
| Publisher: |
IJCIRAS |
| ISSN: |
2581-5334 |
| Volume / Issue: |
Volume 2 Issue 9 |
| Pages: |
9
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| Published On: |
2/19/2020 8:51:46 PM (MM/dd/yyyy) |
| PDF Url: |
http://www.ijciras.com/PublishedPaper/IJCIRAS1520.pdf |
Main Author Details
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Name:
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Olabimtan Olabode Hakeem |
| Institute: |
National Research Institute for Chemical Technology Zaria Kaduna State, Nigeria |
Co - Author Details
| Author Name |
Author Institute |
| Aboki Mahmoud .A |
Scientific and Industrial Research Department, National Research Institute for Chemical Technology Zaria Kaduna State, Nigeria |
| Okibe patience.O |
Department of Industrial and Environmental Pollution, National Research Institute for Chemical Technology Zaria Kaduna State, Nigeria. |
| Ashade Noah.O |
Research and Development, Outstation Coordination Department, National Research Institute for Chemical Technology Zaria Kaduna State, Nigeria. |
| Abubakar Zaid |
Department of Engineering Materials Research, Nigerian Building and Road Research Institute North West Zonal Office, Kano State, Nigeria. |
| Abdulkarim Yahaya. M |
Textile Technology Department, National Research Institute for Chemical Technology Zaria Kaduna State, Nigeria. |
| Opeyemi Adegboyo.O |
Department of Science Laboratory Technology, Federal Polytechnic Ilaro Ogun State, Nigeria. |
| Yahaya yakubu |
Department of Applied Chemistry, Kaduna Polytechnic, Kaduna State, Nigeria. |
Abstract
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Research Area:
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Earth sciences & Allied Sciences |
| KeyWord: |
Magnetic nano-adsorbent, tetra-ethyl orthosilicate, iron oxide Nano-particles, lead, and magnetic field |
| Abstract: |
Lead as one of the toxic and dangerous heavy metals will always require an approach that is cost-effective, simple and environmentally benign to eliminate it from potable water sources especially. Tetra-ethyl orthosilicate was employed as a stabilizing and modifying agent on iron oxide magnetic nano-adsorbent from ferric and ferrous chlorides as precursors. Fourier transform infrared (FT-IR) and Transmission electron microscopy (TEM) was adopted in the characterization of this silica-coated magnetic iron oxide nano-adsorbent (Si-Fe3O4 Nanoparticles). FTIR clearly ascertained the relevant absorption peaks and affirmation of spheroidal Si-Fe3O4 nano-adsorbent at a 20nm nanometer scale with TEM and image J particle analysis software. The actual dimension of 82.54nm or 68.56nm was deduced from the absolute average area of (5756.144 ± 1055.833) nm2; standard error of 333.884nm2 with the silica-coated magnetic nano-adsorbent (Si-Fe3O4) and (77.5 ± 9.24) nm2 and standard error of 2.922nm2 with the uncoated nanoparticles (Fe3O4) were estimated. They (Si-Fe3O4 and Fe3O4) retained polydispersity indices of 2504.800 and 67.811 respectively, characterizing the nano-adsorbent as a polydispersed, randomly oriented nanoparticles. Si-Fe3O4 as a nano-adsorbent was then employed for the adsorption of lead (Pb2+) ions from the aqueous solution of 0.06M and 20mg of lead nitrate [Pb(NO3)2] under the influence of an external magnetic field. Qualitative determination of lead with a test kit was adopted as a direct signal in detecting the presence and absence of lead ions in aqueous solution. It was logically estimated that 20mg/g adsorption capacity of 5g and 100% removal efficiency of Si-Fe3O4 nano-adsorbent were achieved with lead ion. |
Citations
Copy and paste a formatted citation or use one of the links to import into a bibliography manager and reference.
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IEEE
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Olabimtan Olabode Hakeem, Aboki Mahmoud .A, Okibe patience.O, Ashade Noah.O, Abubakar Zaid, Abdulkarim Yahaya. M, Opeyemi Adegboyo.O, Yahaya yakubu, "ADSORPTION OF LEAD IONS (PB2+) FROM AQUEOUS SOLUTION WITH TETRA-ETHYL ORTHOSILICATE MODIFIED SILICA-IRON OXIDE (SI-FE3O4)MAGNETIC NANO-ADSORBENT.", International Journal Of Creative and Innovative Research In All Studies,
vol. 2, no. 9, pp. 26-34, 2020.
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MLA
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Olabimtan Olabode Hakeem, Aboki Mahmoud .A, Okibe patience.O, Ashade Noah.O, Abubakar Zaid, Abdulkarim Yahaya. M, Opeyemi Adegboyo.O, Yahaya yakubu "ADSORPTION OF LEAD IONS (PB2+) FROM AQUEOUS SOLUTION WITH TETRA-ETHYL ORTHOSILICATE MODIFIED SILICA-IRON OXIDE (SI-FE3O4)MAGNETIC NANO-ADSORBENT.." International Journal Of Creative and Innovative Research In All Studies,
vol 2, no. 9, 2020, pp. 26-34.
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APA
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Olabimtan Olabode Hakeem, Aboki Mahmoud .A, Okibe patience.O, Ashade Noah.O, Abubakar Zaid, Abdulkarim Yahaya. M, Opeyemi Adegboyo.O, Yahaya yakubu (2020). ADSORPTION OF LEAD IONS (PB2+) FROM AQUEOUS SOLUTION WITH TETRA-ETHYL ORTHOSILICATE MODIFIED SILICA-IRON OXIDE (SI-FE3O4)MAGNETIC NANO-ADSORBENT.. International Journal Of Creative and Innovative Research In All Studies,
2(9), 26-34.
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ADSORPTION OF LEAD IONS (PB2+) FROM AQUEOUS SOLUTION WITH TETRA-ETHYL ORTHOSILICATE MODIFIED SILICA-IRON OXIDE (SI-FE3O4)MAGNETIC NANO-ADSORBENT.
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